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Introduced March 2006
Features Summary
MultiSYNTH Features
| Features | Single-mode format | Multimode format |
|---|---|---|
| Volume working range | 1 vial, 0.2 to 40 mL | 12 vials, 0.2 to 40 mL |
| Contact-less temperature control | Yes, by infrared | Yes, sequentially by infrared in each vial |
| Direct temperature control | Yes, by fiber-optic | Yes, by fiber-optic in a reference vessel |
| Pressure control | Yes, built in to reaction vial's safety valve | Yes, built in to all vials |
| Magnetic stirring | Yes | Yes, in all vials |
| Shaking | Yes | Yes, in all vials |
| Fast cooling | Yes, by compressed air | Yes, sequentially by compressed air |
Available Reaction Vials
| Single-mode format | |||||
|---|---|---|---|---|---|
| Type | Material | Volume | Working volume | Max. temperature | Max. pressure |
| Reflux | Glass | Up to 1,000 mL | Up to 500 mL | 250°C | Reflux |
| PRO | TFM | 70 mL | Up to 35 mL | 200°C | 30 bar |
| Standard large vial | Glass or quartz | 10 mL | Up to 5 mL | 200°C | 20 bar |
| Standard medium vial | Glass or quartz | 5 mL | Up to 2.5 mL | 200°C | 20 bar |
| Standard small vial | Glass or quartz | 2 mL | Up to 1 mL | 200°C | 20 bar |
| Multimode format | ||||||
|---|---|---|---|---|---|---|
| Type | Number of vials | Material | Volume | Working volume | Max. temperature | Max. pressure |
| Standard large vial | 12 | Glass or quartz | 10 mL | Up to 5 mL | 200°C | 20 bar |
| Standard medium vial | 12 | Glass or quartz | 5 mL | Up to 2.5 mL | 200°C | 20 bar |
| Standard small vial | 12 | Glass or quartz | 2 mL | Up to 1 mL | 200°C | 20 bar |
| PRO | 10 | TFM | 70 mL | Up to 35 mL | 200°C | 30 bar |
Technical Specs
Microwave Hardware
- Single-magnetron system with homogeneous microwave distribution in the cavity.
- Installed power 800 watt.
- Output power 800 watt, controlled via microprocessor.
- User-selectable continuous or pulsed microwave emission.
- Single-mode and multi-mode setup for batch or parallel synthesis.
- Easy access to the microwave cavity by fully automated opening/closing top housing.
- Compact microwave cavity 26.5 x 24.5 x 20.0 (h) cm, for high microwave density.
- Microwave cavity entirely made of 18/8 stainless steel housing with multi-layer PTFE plasma coating applied at over 350°C.
- All hardware protected against acids/organic solvents with polymer coating both on inside and outside surfaces.
- Built-in exhaust system, located in the side of the cavity, separate from electronics to prevent corrosion.
- Built-in airflow system, for rapid vial cooling and reaction quenching.
Reaction Sensors
- Direct temperature monitoring and control via fiber-optic probe up to 300°C in a reference vessel.
- Contact-less temperature monitoring and control via infrared up to 300°C in all vessels.
User Interface
- Industrial grade touch-screen controller. 6.5 in. screen with 65,000 colors.
- VGA resolution 640x480 for sharp process graphics.
- 1 USB port to connect printer, 2 PS2 ports for mouse and keyboard, 3 RS 232 ports for external devices.
- Methods and runs saved on Windows-compatible removable flash-card.
Measurements
- Weight ~ 68 kg.
- External dimensions 47.5 x 68.0 x 52.0 (h) cm (closed); 96.0 (h) cm (open)
- Power 220V/50–60Hz, 2.0 kW.
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