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U.S. EPA Methods

EPA Method 7473: Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrophotometry
Method 7473 is designated for the determination of mercury in solids, aqueous samples, and digestion solutions, in both the laboratory and field environments. Integration of thermal decomposition, sample preparation, and atomic absorption detection reduces the total analysis time of most samples to less than five minutes, in either the laboratory or field setting.
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ASTM (American Society of Testing and Materials) Methods

ASTM D-6722-01
Standard Test Method for Total Mercury in Coal and Coal Combustion Residues by Direct Combustion Analysis

The above method can be downloaded for a fee at http://www.astm.org.

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