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SRC MICROWAVE DIGESTION OF HEAVY CRUDE OIL FOR TRACE METALS ANALYSIS BY ICP-OES

Compared to traditional ashing, acid digestion using SRC has been found to be significantly faster, avoids the risk of airborne contamination, and retains volatile elements in solution prior to analysis by ICP-OES.  Milestone’s UltraWAVE addresses these uses and offers increased sample throughput.

pdfSRC OIL APP NOTE (Click To Download)

Summary-Benefits of SRC Technology PDF Print E-mail

Superior Performance

  • Precise temperature and pressure control on every sample
  • Superior digestion quality
  • Higher sample weights can be digested
  • Minimal sample handling – less contamination risk
  • Less digestion acid is used (typically 2-4mL) – lower blank levels
  • Reference materials can be digested with samples: in-run digestion QC

Increased Productivity, Lower Operating Cost

  • Reaction vessel assembly and disassembly steps eliminated
  • Operator time is significantly reduced – by up to 4x
  • Separate microwave run to clean vessels (as with closed vessel digestion) is eliminated
  • Max. sample capacity: 15 (UltraWAVE), 40* (UltraCLAVE)
  • Multiple sample matrices and acid chemistries digested in the same run – no “batching” of samples
  • Standard, disposable glass vials (or reusable quartz vials) are used
  • Reaction vessel consumables (vessel/cap/shield) costs eliminated

UltraCLAVE has an optional rack that holds 77 x 12mL vials. While 12mL vials are slightly too small for some sample types, they work well for microsampling applications such as clinical; and in these cases, 77 samples can be digested simultaneously.